Justus Liebig s Annalen der Chemie

Article . 1969 . Peer-reviewed

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Darstellung und Hydrolyse von 4‐Halogenmethylen‐1.3‐dioxolanen

Name: Darstellung und Hydrolyse von 4‐Halogenmethylen‐1.3‐dioxolanen
Creator: Herbert Meister

descriptionPublicationkeyboard_double_arrow_right Article 09 Jul 1969 English Publisher:WileyJournal:Justus Liebigs Annalen der Chemie, volume 724, pages 128-136 (issn: 0075-4617,

Authors: Herbert Meister;

doi: 10.1002/jlac.19697240115

Darstellung und Hydrolyse von 4‐Halogenmethylen‐1.3‐dioxolanen

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Abstract

AbstractDurch basenkatalysierte Addition von Formaldehyd an 1‐Halogen‐propin‐(1)‐ole‐(3) (3) werden 4‐Halogenmethylen‐1.3‐dioxolane (4a–o) erhalten. Die saure Hydrolyse von 4 führt zu 1‐Halogen‐propanol‐(3)‐onen‐(2) (5a–f, i–o). Soweit diese eine primäre oder sekundäre Hydroxy‐Gruppe enthalten (5a–f), werden sie beim Erwärmen in die 2.3‐Diketone 6 bzw. 7a–c und Halogenwasserstoff gespalten.

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Darstellung und Hydrolyse von 4‐Halogenmethylen‐1.3‐dioxolanen

Darstellung und Hydrolyse von 4‐Halogenmethylen‐1.3‐dioxolanen

2 Research products, page 1 of 1

Microwave assisted synthesis of ring junction heterocyclic antioxidants

Three-Component Synthesis of 2-Amino-3-cyano-4H-chromenes, In Silico Analysis of Their Pharmacological Profile, and In Vitro Anticancer and Antifungal Testing