Synthesis and Properties of Bimetallic Alkoxides and Mixed Acetylacetonates of Tin(II) with Aluminium (III)

descriptionPublicationkeyboard_double_arrow_right Article 01 Jan 1981 English Publisher:Informa UK LimitedJournal:Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, volume 11, pages 345-359 (issn: 0094-5714, eissn: 1532-2440,

Authors: R. C. Mehrotra; R. R. Goyal; N. C. Jain;

doi: 10.1080/00945718108055987

Synthesis and Properties of Bimetallic Alkoxides and Mixed Acetylacetonates of Tin(II) with Aluminium (III)

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Abstract

Abstract Evidence for the formation of a bimetallic isopropoxide of tin(II) with aluminium (III) has been obtained by conductance studies. The compound (I), Sn [Al(OPr1)4]2, has been synthesised, purified and characterized. Chemical evidence for the formation of compound (I) was obtained by reacting Sn[Al(OPr1)4]2 with acetylacatone. A number of other bimetallic derivatives, Sn[Al(OR)4]2 and Sn[Al(OPr1)(oBut)3]2 (where R = Me, Et, CF3CH2 and (CH2Cl)2CH) have also been synthesised by the alcohol interchange technique. All these compounds were characterisad by i.r. and p.m.r. spectral studies. The molecular weights of these compounds in boiling benzene have also been determined.

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University of Delhi
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University of Rajasthan
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